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Nicotine solution must be shaken to avoid hotspots, is this true when using 55 gallon drums?
submitted over 6 years ago by absolutelychocolate

Just recently started working for a manufacturer, I noticed our mixologist uses an electric pump to pump nicotine and vg into 5 gallon buckets from 55 gallon drums. I brought up to him that nicotine needs to be shaken periodically to avoid hotspots. He said that that's only the case with small quantities because the hotspots are small and don't really effect the outcome when mixing in the volumes we mix in.

Is this true? If it's not, I really don't see how we could shake a 55 gallon drum as it weighs like 500 pounds.

They've been in business for many years and have never had a complaint so based off that I guess what he says is true, just curious.

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6 points
 
by MarathonTortoiseover 6 years ago

Never had experience with that huge amount of Nicotine, but based off what the mixologist says, it kinda makes sense.

Home Hobbyists don't go through that much nic, hell I just bought 150ml of 100mg nic salts, and I probably won't need to buy more for a long time.

I bet the electric pump also aides in mixing the nicotine. When the nicotine is put into smaller bottles, I would be that's when you would be more focused on hot spots.

6 points
 
by squiredover 6 years agoMixologist

Just FYI, you don't want to shake nic, you want to stir it. Shaking it introduces bubbles into the solution and hastens oxidation.

3 points
 
by absolutelychocolateover 6 years ago

good to know, but im sure that wouldnt really matter to him because I've seen him go through 2 55 gallon drums of it in a day so he's using it up faster than it would oxidize

4 points
 
by juthincover 6 years agoI improved Grack and all I got was this lousy flair

The drums would get agitated some just gettng them into position, the pump would induce currents inside the drum, etc. And yeah, it likely averages out a lot, and the finished mix will be uniform in distribution of all compounds if they use the right ewuipment.

2 points
 
by absolutelychocolateover 6 years ago

makes sense, thanks

2 points
 
by DGsirb1978over 6 years ago

TBH, I think hotspots is overblown even in DIY in my experience. I’ve been good about mixing, but I’ve never actually seen anyone deal with hotspots.

1 points
 
by IWillKarateKickYouover 6 years ago

Ya going through them that fast I imagine keeps it pretty mixed with the pump causing some constant disturbance to the drum. I would be a little worried about coming in the next morning to the drum thats been sitting all night but as far as the levels of hotspots I wouldnt imagine it would get up to 200mg/ml in one spot or anything but there are probably slight level differences in spots

2 points
 
by iLLNiSSover 6 years ago

If the bottle comes sealed with nitrogen shake the fuck out of it, won’t make a difference. It’s only after you open it, shake it, open it, shake it, you should be worried.

3 points
 
by squiredover 6 years agoMixologist

True that. You can also buy argon gas as wine saver for the same purpose.

2 points
 
by MiLlIoNs81over 6 years agoDiketones, Schmiketones

I just ordered some today from Amazon, found link in a 3y old post on here. $10 for piece of mind with our nic is well worth it.

1 points
 
by thelateoctoberover 6 years ago

Yeah that's why I decant my nic into 30 ml bottles, so I can shake the shit out of it and not worry about it. I go through it fast enough it would probably be fine in the 120ml bottle it comes in.

1 points
 
by cloud1eover 6 years ago

Shake unsteeped juice you wanna vape soon

4 points
 
by scorp00over 6 years ago

A long paint mixer that attaches to a drill could stir it all up quickly.

2 points
 
by chemchemqover 6 years ago

What kind of PPE are you using? Pure nicotine is risky stuff. If not using full ventilation containment on that scale you need proper gear

3 points
 
by absolutelychocolateover 6 years ago

its 100mg/ml

1 points
 
by chemchemqover 6 years ago

Oh that’s not so bad then, I use pure nic!, bit more scary

2 points
 
by doofus__mcgoofusover 6 years ago

That scares the $#!+ out of me... Be careful and don’t end up in the news!

1 points
 
by IWillKarateKickYouover 6 years ago

10x more scary!

1 points
 
by absolutelychocolateover 6 years ago

is pure nicotine a liquid? I always assumed it was like a solid crystal or something

2 points
 
by chromedomeomeover 6 years ago

I would think to stir up a 55g drum you just need one of those 2-3 foot mixing poles you can attach to a power drill. Or just use like a rubber paddle

1 points
 
by broslikethisover 6 years ago

Done some larger scale manufacturing - we always mixed the nic after transferring it to 2.5 gallon jugs. We just shook it. I could understand the concern about wanting to mix it up before transferring to smaller containers but this is just how I was always is taught to do it and we never had complaints.

Two 55 gal drums in a day though, damn, that's some large scale. Do you mind if I ask, how much of your process is automated? All the flavor mixing I assume is done by hand, your bottle labeling, filling, capping, and safety-sealing though, is that all automated?

3 points
 
by absolutelychocolateover 6 years ago

We have 2 machines and are getting a third. one machine does 30ml plastic bottles the other does 100ml plastic bottles. the third machine we're getting will do 60ml plastic bottles.

each machine fills, caps, and labels. the machines each require 2 people, one to load bottles and caps and the other to collect the bottles. They have me loading the bottles and caps right now.

The machines sometimes fuck up a bottle cap or a label so there's three people who do quality check and fix bad bottles before they go on the shelf.

1 points
 
by St1llFrankover 6 years ago

Thank's for your insights. I always wondered how some of that stuff was done. I also couldn't imagine how much liquid was being made. 2 x 55gallon drums of nic in a day. That's a lot. I don't even want to try doing the math lol.

2 points
 
by absolutelychocolateover 6 years ago

well it's not as much as you may think. They are drums of nicotine salts at 100 mg/ml. Making 25 and 50 mg juice so half the volume of each 5 gallon bucket is nicotine salts.

the freebase nicotine comes in single gallon jugs and we use comparatively a lot less of that than we do nicotine salts.

1 points
 
by Stratocraticover 6 years ago

>If it's not, I really don't see how we could shake a 55 gallon drum as it weighs like 500 pounds.

Yeah, I don't know of anything large enough to shake it. Stirring might mix it well enough, but you'd have to be able to reach all the way to the bottom. The company I worked for used a drum roller. Most things would be rolled for an hour or more, depending on the carrier (VG vs. PG).

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